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A Bond That Should Never Be Broken: Adhesion and Other Failures in Hot Fluid-Applied Rubberized Asphalt Membranes

May 15, 2013

4 • I n t e r f a c e M a y / J u n e 2 0 1 3
INTRODU CTION
This paper presents case studies of failures
in the application of hot fluid-applied
rubberized asphalt in new construction,
discusses possible causes of failure, and
discusses how the design and construction
teams on each project overcame the challenges
they encountered. The authors will
demonstrate that a combination of thorough
field observation, construction of mock-ups,
and application of available ASTM testing
methods to determine acceptability of the
substrate will provide the best chance at
successful application of hot fluid-applied
rubberized-asphalt membranes.
A BRIEF HISTORY
Hot fluid-applied rubberized-asphalt
membranes have been used in the roofing
and waterproofing industries for decades.
Their failure is not a new phenomenon in
the waterproofing industry but is uncommon
when compared to the failure rates
of other waterproofing membranes. The
industry has adjusted the membrane over
time to accommodate failures observed in
the overall system. Excess moisture vapor
in concrete substrates can adversely affect
fluid-applied waterproofing membranes due
to their initial application, and this phenomenon
has influenced the evolution of
hot fluid-applied rubberized asphalt.
Initially, hot fluid-applied rubberized-asphalt
roofing was commonly installed in a
single, 180-mil layer over concrete decks.
A slew of failures in the mid-1980s–particularly
on projects that utilized lightweight
structural concrete as a substrate–led manufacturers
to reevaluate their assembly.
Lightweight concrete typically requires a
longer drying time in comparison with normal-
weight concrete, due to the increased
absorption properties of the lightweight
aggregates. At the projects that experienced
failures during installation, the applicators
observed extensive pinholing after application
of the single layer of hot fluid-applied
rubberized asphalt. The pinholing was
caused when moisture in the concrete deck
vaporized and moved to the exterior through
the freshly applied hot fluid-applied rubberized-
asphalt membrane.
The industry responded to the failures
with the addition of a reinforcing layer and a
second coat of membrane. After the 1980s,
an increasing number of hot fluid-applied
rubberized-asphalt systems consisted of
a 215-mil-thick coating with fabric reinforcing,
in part to compensate for the high
moisture condition in lightweight concrete
substrates. Revised specifications for the
215-mil system included a two-part installation.
The first 90-mil-thick layer of hot
rubberized asphalt and fabric allows for and
isolates the expected pinholing effect. The
subsequent application of a 125-mil layer
fuses with the initial layer, consolidating to
form the complete assembly.
MODE S OF FAILU RE
The addition of reinforcement into the
hot fluid-applied rubberized-asphalt system
to overcome the pinholing enhanced the
overall system and reliability as a waterproofing
membrane. However, despite the
evolution of hot fluid-applied rubberized
asphalt into a thicker reinforced system, the
industry still observes failures, including
delamination and pinholing. These modes of
failure are described in greater detail below.
Failure to Initially Adhere to Substrate
Low-permeability roofing systems (e.g.,
hot fluid-applied rubberized asphalt) can
blister or delaminate at the concrete deck
substrate due to a vapor drive toward the
roofing or waterproofing assembly, improper
surface preparation, or other sources.1
Delamination can occur when the internal
pressure exerted by a water vapor or solvent
vapor (result of primer application) exceeds
the bond forces between the membrane and
the substrate. The membrane can also fail
to initially bond to the substrate, causing
delamination if the substrate is too smooth
or includes a bond inhibitor (e.g., concrete
additive or curing compound; see additional
discussion below). When heated by the sun,
hot fluid-applied rubberized asphalt can
This article is reprinted from the RCI Building Envelope Technology Symposium, October 10-11, 2011, in Charlotte, NC.
become soft and pliable. If the membrane
is not fully adhered, it will delaminate from
the substrate. Upon cooling, the blistered
or delaminated area remains plastically
deformed and, on reheating, can expand
further. If left uncorrected, the delamination
can lead to building leakage.
Pinholing
When the vapor drive through the
membrane is strong enough during initial
application of the membrane, fluid-applied
waterproofing membranes develop small
discontinuities that resemble pinholes prior
to curing. The areas of discontinuity are
gaps in the membrane and are often circular
in shape. The gaps then become
potential water-entry locations after the
membrane sets. Hot fluid-applied rubberized
asphalt also develops pinholes due to
excess moisture within the concrete substrate
as it vaporizes and drives through the
uncured membrane. As discussed above,
the industry addressed this issue with the
addition of reinforcement and a second
layer of membrane.
Interlayer Adhesive Failure
Some blisters in the membrane can form
between the reinforcing sheet and the second
layer of hot-applied asphalt membrane.
These blisters can form if an unknown
substance or moisture is present on the
surface of the reinforcing sheet at the time
of application.
TESTS AND PRACTICES TO PREVENT
FAILU RE
Our experience shows that successful
application of hot-applied rubberized
asphalt is highly dependent on the age and
moisture content of the concrete substrate,
well-timed application of the membrane,
and a project-specific series of adhesion
tests to determine proper primer coverage.
Moisture in Concrete
Manufacturers of hot fluid-applied rubberized
asphalt typically recommend applying
the membrane to a substrate that is
clean, dry, and free of water, ice, snow,
dust, curing compound, or any foreign
matter. Concrete should be allowed to cure
for a miniumun of 14 days (21 for lightweight
concrete). Cure time is essential
to allow water to dissipate from the concrete.
Several test methods are available to
address moisture in concrete decks prior
to the application of a hot fluid-applied
rubberized-asphalt membrane. Each test
method described below measures moisture
content of the concrete substrate. If used
properly, these tests can indicate whether
a concrete deck is too moist to support the
application of a hot fluid-applied asphalt
system.
• ASTM D4263 – Standard Test
Method for Indicating Moisture in
Concrete by the Plastic Sheet Method.
This test consists of sealing a piece
of plastic sheeting (approximately
18 in. by 18 in.) to the concrete surface
(Figure 1). After approximately
16 hours, the sheet is removed,
and both the sheet and concrete
surface are inspected. Moisture on
either the plastic or concrete surface
indicates wet concrete, which
requires additional drying time prior
to installation of a hot fluid-applied
rubberized-asphalt membrane.
ASTM D4263 requires testing of one
area per 500 sq. ft. maximum. This
test has several limitations; the exterior
environment (i.e., temperature,
amount of direct sunlight or shade,
etc.) can greatly impact the results of
this test.
• ASTM F2170 – Standard Test Method
for Determining Relative Humidity in
Concrete Floor Slabs Using in situ
Probes. The test includes two methods
of placing probes in a concrete
slab; the first involves drilling a hole
in the concrete slab after placement
and inserting a plastic sleeve, while
the other involves forming a hollow
sleeve in the slab and placing
the concrete around it. The sleeve
allows for placement of probes that
measure relative humidity at a specific
depth within the concrete slab.
The plastic sleeves are covered and
sealed to the concrete deck throughout
the entire test to prevent any
changes to the air in the sleeve.
By measuring the relative humidity
of the slab, the user can predict
the success or failure of a coating
applied to the surface of the concrete
due to excessive moisture content.
• ASTM F2420 – Standard Test
Method for Determining Relative
Humidity on the Surface of Concrete
Floor Slab Using Relative Humidity
Probe Measurement and Insulated
Hood. Similar to ASTM F2170, this
test method measures the percent of
relative humidity above the surface
of a concrete slab. By placing an
insulated hood that contains humidity-
measuring apparatus, the user
can predict whether the moisture in
the concrete will allow for the placement
of a coating on the surface
of the concrete. This test, however,
does not predict moisture movement
or overall moisture content of the
slab, since it measures surface relative
humidity only. Moisture within
concrete is dynamic and can cause
M a y / J u n e 2 0 1 3 I n t e r f a c e • 5
Figure 1 – ASTM D4263 is used to test for the presence of moisture in a concrete slab.
6 • I n t e r f a c e M a y / J u n e 2 0 1 3
failures of a waterproofing membrane
under conditions that differ
from what the moisture probe measures.
Primer Application
In addition to gauging the moisture in
the concrete substrate, manufacturers have
long used asphalt-based primers to enhance
the bond between the concrete surface
and hot fluid-applied rubberized-asphalt
membranes. These primers must conform
to ASTM D41-11 – Standard Specification
for Asphalt Primer Used in Roofing,
Dampproofing, and Waterproofing, and are
applied in a thin layer over the concrete
substrate using a brush, roller, or spray
equipment. Coverage rates can vary between
100 and 600 sq. ft./gal., depending on
porosity and surface
texture of the
substrate and the
selected primer. When applied too thickly,
primers can experience increased drying
times or not cure by the time the membrane
is applied; when applied too thinly, primers
may not adequately cover the substrate.
Additionally, primers can feel dry to touch
but the solvent in the primer might not have
fully flashed off. In all cases, the membrane
may experience reduced adhesion to the
deck.
Applicators must also pay careful attention
to duration of exposure of the primer
to weather and construction traffic. Primers
left overnight can accumulate moisture in
the form of dew or pick up dirt and debris
from construction traffic. In addition to the
challenges associated
with application
of the primer,
m a n u f a c t u r e r s
have reformulated primers to produce fewer
volatile organic compounds (VOCs) to make
them greener” and comply with legislation.
These alternative primers have a short
track record and therefore cannot be directly
correlated to adhesion failures in the
membrane. Therefore, the designer should
require careful evaluation of the primer,
preferably through mock-ups, to evaluate
the effectiveness and suitability prior to
selection and wholesale installation.
Surface Preparation
Construction of mock-ups will demonstrate
whether any concrete admixtures,
curing compounds, or concrete finishes
will affect the bond of the hot fluid-applied
rubberized-asphalt membrane to the
concrete deck. Many admixtures have no
effect, but some curing agents may prevent
Figure 2 – Both mock-ups demonstrating pinholing.
The mock-up to the left is acceptable, while the
mock-up below has excessive pinholing.
Figures 3A and 3B – The mock-up to the right shows an
adhesive failure in which the hot fluid-applied rubberized
asphalt pulls completely away from the concrete substrate. The
mock-up above demonstrates a more desirable cohesive failure.
a strong bond from forming between the
waterproofing membrane and the surface
of the concrete. Manufacturers require concrete
substrate to have a wood or broom
finish. The finish can also affect the bond
between the membrane and the substrate. A
steel-troweled finish or a smooth finish from
formwork can inhibit the bond, whereas a
broom or wood-float finish will enhance the
bond. A lack of bond between the waterproofing
membrane and concrete deck due
to the presence of a concrete admixture can
be easily fixed by using an etching agent or
other chemical agent on the surface of the
concrete deck. Mechanical abrasion (i.e.,
sandblasting, shotblasting, diamond grinding,
etc.) will enhance the bond in areas
with poor adhesion due to the presence of a
curing compound or smooth finish.
Construction Mock-ups
By building mock-ups, a construction
team can evaluate which combination of
products and coverage rates creates the best
adhesion on a case-by-case basis. Without
determining which balance of materials
is correct for a particular application, the
result could be widespread adhesive failure
of the waterproofing membrane.
The moisture content and the condition
of the concrete deck can vary based
on the area and exposure of the project.
Constructing mock-ups at each area of
application will best predict success or failure
of the membrane and indicate whether
primer rates should vary from area to
area. A hot fluid-applied rubberized-asphalt
mock-up must meet the following criteria to
confirm adequate adhesion:
• The mock-up must produce little to
no pinholing (Figure 2). If the project
team first conducts moisture
tests on the concrete, such as those
described above, pinholing of the
mock-up will be less likely.
• The mock-up must demonstrate
cohesive failure of the waterproofing
membrane. A cohesive failure means
the membrane, when placed under
stresses great enough to cause tearing,
will debond from itself rather
than the substrate. An adhesive
failure, where the membrane tears
away from the substrate rather than
itself, is less desirable and is indicative
of a higher risk of delamination.
To perform an adhesion test, a small
area of hot fluid-applied rubberized
asphalt is placed with a reinforcing
strip of fabric or neoprene embedded
in it and a pull tab left exposed on
the end (Figure 3). The fabric or neoprene
is pulled until the membrane
fails by tearing. A cohesive failure
indicates the bond to the concrete
deck is stronger than the internal
bond between layers of membrane,
while an adhesive failure indicates
insufficient bond between the membrane
and the deck. Different test
methods can measure numerical
adhesion values for comparison purposes,
but the main objective of the
test is to determine mode of failure.
CASE STUD IES
The following case studies provide greater
detail on a few projects that demonstrated
adhesion issues with the hot fluid-applied
rubberized-asphalt system.
CASE STUD Y NO. 1: CURING AGENTS
Background
A biosciences building located in
Northern California featured application
of a hot fluid-applied rubberized-asphalt
membrane on a large podium area at
grade and multiple levels of vegetative roof
in a protected membrane configuration
(Figure 4).
M a y / J u n e 2 0 1 3 I n t e r f a c e • 7
Figure 4 – Hot fluid-applied rubberized-asphalt application on a project in Northern
California.
8 • I n t e r f a c e M a y / J u n e 2 0 1 3
Problem 1
Initial application of the hot fluidapplied
rubberized-asphalt system began at
the podium level. To meet the project schedule,
the construction team used a concrete
curing agent prior to application of the hot
fluid-applied rubberized-asphalt membrane.
Despite meeting the concrete admixture
manufacturer’s curing requirements, the
initial application of primer and membrane
easily delaminated from the surface of the
concrete deck. In response, the construction
team used a concrete surface treatment to
negate the effects of the concrete admixture.
Adhesion problems persisted.
Solution 1
The team discerned that the
membrane delaminated under certain
coverage rates of primer. The
team devised a series of mock-ups to
determine the optimal primer coverage,
utilizing varying coverage rates
and adhesion tests. Through the
mock-up process, it became apparent
a super-thin film of primer allowed
the hot fluid-applied rubberized-asphalt
membrane to fully bond to the
concrete substrate.
Problem 2
During later installation of the
same hot fluid-applied rubberized-asphalt
membrane on the vegetative
roof assembly, the membrane experienced
extensive pinhole failures.
Solution 2
After reviewing the installer’s primer
application procedures and determining
that they matched the successful application
at the podium deck below, it became
clear that another mechanism of failure
was causing the pinholing. Upon closer
examination, the construction team discovered
that the pinholes occurred only in
the top coat of the membrane (Figure 5). In
reviewing its application procedures, the
team realized that the installers allowed the
bottom coat and reinforcing to sit overnight.
Upon cooling during the nighttime hours,
the reinforcement collected moisture from
the air. The moisture on the surface of the
reinforcement vaporized and drove through
the second layer of hot fluid-applied rubberized
asphalt upon its application the
next morning. The construction team concluded
that a well-timed application of the
complete waterproofing assembly is critical
to adhesion and overall performance of the
membrane. At areas of concern, the team
allowed the second layer to thoroughly dry
and then applied a third coat over the area
with extensive pinholing. For the remainder
of the project, the waterproofing contractor
installed only as much material as could be
covered with the second layer of membrane
in a single day.
CASE STUD Y NO. 2: BLISTERS IN
MEMBRANE
Background
The second case study occurred during
the construction of a new hospital in
Southern California. The project included a
60,000-sq.-ft. vegetative roof over the operating
rooms (Figure 6). The concrete deck is
a 5-in.-thick, normal-weight concrete over
a vented steel deck. The concrete cured for
approximately four months prior to application
of the hot fluid-applied rubberized-asphalt
membrane. The installer reviewed the
curing compounds, form-release agents,
and substrate preparation with the hot
fluid-applied rubberized asphalt manufacturer
prior to the start.
As outlined in the specifications, the
installer prepared a mock-up of the installation,
including all unique conditions, per-
Figure 5 – Pinholing through the top layer of fluid-applied rubberized asphalt.
Figure 6 – A hot fluid-applied rubberized-asphalt vegetative roof in Southern California.
formed moisture tests using the plastic sheet method, and
later performed ten adhesion tests approximately halfway
through the installation of the hot fluid-applied rubberized-asphalt
membrane. The project team observed good adhesion
(cohesive failure) at all adhesion tests in the field of the roof.
Problem 1
Adhesive failure occurred between the membrane and the
concrete substrate at the two test cuts performed at the parapets
(Figures 7A and 7B).
Solution 1
After reviewing the application process
and the differences between the deck and
the parapet walls, the team attributed the
poor adhesion to surface preparation. The
parapet walls were finished smooth (not
the recommended broom or wood-trowel
finish). The team constructed a mock-up
with varying degrees of surface preparation,
including light application of surface
primer, wire wheel, and bead blasting. The
wire wheel provided the best adhesion. To
remediate the areas already completed, the
contractor removed the protection sheet,
scraped off the membrane, wire-wheeled
the concrete, and then wire-wheeled the
concrete again with a clean wheel. The
contractor then installed the reinforced hot
fluid-applied rubberized-asphalt membrane
over a primed concrete wall.
Problem 2
Shortly after the contractor completed
installation of the second half of the roof,
the project team performed random adhesion
tests throughout the installation. At
the two areas selected, we observed large
blisters in the hot fluid-applied rubberized-
asphalt membrane. The delamination
M a y / J u n e 2 0 1 3 I n t e r f a c e • 9
Figures 7A and 7B – Adhesive failure at parapets.
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1 0 • I n t e r f a c e M a y / J u n e 2 0 1 3
occurred between the hot fluid-applied rubberized
asphalt and the concrete deck and
between layers of hot fluid-applied asphalt
(Figures 8A and 8B).
Solution 2
To confirm the levels of moisture in the
concrete deck, the project team performed
relative humidity tests using in situ probes.
The team drilled ten holes at random locations
in the concrete deck at varying depths
and measured the moisture content. In each
location, the moisture content was below
76.9%, with an average of 72.7% relative
humidity. Typically, an average relative
humidity of 75%, and below indicates that
moisture in the concrete deck is not the
source of failure.
The team narrowed the source of blistering
to either improper drying time of the
primer or an unknown substance on the
concrete deck (e.g., perhaps a substance
spilled on the deck during construction or
someone tracked something on their shoes
across the deck). Through additional adhesion
testing, the team identified the area of
blisters to an approximately 2,400-sq.-ft.
area—a much smaller area than the entire
application of membrane on the project. The
installer then removed the protection sheet,
cut open the blisters down to the concrete
deck, and patched them with the hot fluid-
applied rubberized-asphalt system (215-
mil reinforced system), extending the repair
6 inches in all directions. The waterproofing
contractor installed the protection layer set
in an additional 90-mil layer of hot fluidapplied
rubberized asphalt over the entire
area. The waterproofing contractor allowed
the primer to dry for a minimum of 24 hours
on the remaining portions of the project.
Manufacturers typically require application
of the hot fluid-applied rubberized asphalt
over the primer during the same day (within
four to six hours), but the project team
learned in this instance that variance from
this rule produced a better result. In addition,
the cut-and-patch method successfully
solved the blistering encountered during the
first portion of application.
CASE STUD Y NO. 3: PRIMER
APPLICATION RATE
Background
On a project in Northern California, a
20-year-old hot fluid-applied rubberized-asphalt
membrane was experiencing failures
due to a combination of root growth and
aging materials. The project consists of multiple
residences united by a large podium
deck in the center of the structure on the
third floor. The podium deck is covered with
vegetative materials over a protected hot
fluid-applied rubberized-asphalt membrane.
Figures 8A and 8B – Blistering
in the field of the roof at the top;
adhesive failure of test openings in
the field of the roof at the bottom.
Problem
The owner observed leakage through
the concrete slab below the podium deck
into the parking garage below. To remediate
the leakage, the owner sought wholesale
replacement of the waterproofing membrane
above areas experiencing leakage
(Figure 9). After removal of the overburden
and existing waterproofing, the construction
team prepared several mock-ups with
varying primer coverage rates to determine
the amount that would yield the best adhesion
to the concrete deck. Surprisingly, even
the old concrete deck, which after 20 years
should demonstrate a moisture content
at equilibrium, yielded a variety of results
dependent on the coverage of primer.
Figure 9 – Wholesale replacement of an existing hot fluid-applied rubberized-asphalt
membrane still required attention to concrete moisture content and primer application rates.
Figure 10 – The team used mock-ups to find the best primer application rates to cause
adhesion of the membrane.
M a y / J u n e 2 0 1 3 I n t e r f a c e • 1 1
Solution
The construction team selected a primer
coverage rate associated with the mock-up
that had the best adhesion and successfully
used the hot fluid-applied rubberized
asphalt to the repair areas (Figure 10). The
team learned from these mock-ups, though,
that moisture content alone does not dictate
the success or failure of the waterproofing
assembly. Optimal primer coverage rates
vary on a project-by-project basis, and performing
mock-ups to determine the amount
of primer is critical to successful application.
These case studies demonstrate that
failures of hot fluid-applied rubberized
asphalt applied to concrete can be overcome
with forethought and diligence. On each
project, the team recognized the need for
adjustments to the application process and
utilized quality control methods to create a
successful application.
RECOMMENDATIONS
Several tools are available to prevent the
failure of hot-applied rubberized asphalt
to concrete decks. Each tool will help the
user better understand the characteristics
of deck adhesion on a project-by-project
basis. Successful application will involve
the following:
• Allowing the concrete substrate adequate
time to cure
• Measuring the relative humidity of
the deck using one of the available
ASTM test methods
• Properly cleaning the deck, including
surface treatment if concrete
additives are present, and mechanical
abrasion to remove curing compounds
and provide the desired surface
texture
• Constructing several mock-ups at
each area of hot fluid-applied rubberized
asphalt application to establish
the appropriate amount of primer
application, required drying time,
and surface preparation
To prevent future failures, the most
reliable approach is to incorporate the recommendations
outlined above into the specification.
Specifications should include the
following: requirements to perform a specific
number of relative humidity tests on the
concrete substrate prior to application of the
membrane, quantification of the acceptable
moisture content of the concrete substrate,
inclusion of surface treatment for concrete
additives and mechanical abrasion to remove
curing compounds, and construction of several
mock-ups. During construction, mockup
testing and enhanced quality control
procedures will provide the best chance for
a successful application of hot fluid-applied
rubberized-asphalt membranes.
FOOTNOTE
1. Delamination can also occur when
water works against exposed edges of
membrane until the membrane separates
from the deck. Delamination
of this nature is less likely to occur
in the field of membrane application
but is common at edge or transition
locations due to poor detailing. For
the purposes of this article, only
delamination due to vapor drive is
considered.
1 2 • I n t e r f a c e M a y / J u n e 2 0 1 3
Christina T. Parker is a member of the technology staff in
SGH’s Newport Beach, CA, office. She has led many of the
firm’s most notable building technology and historic preservation
projects, including the rehabilitation of the Luzerne
County Courthouse, Pennsylvania’s state capitol, and prepared
an historic structures report for the Arts and Industries
Building. Parker is a guest lecturer for the Structural
Engineering Department at the University of California at
San Diego.
Christina T. Parker
Anthony J. Nicastro, PE, is a senior engineer at national engineering
firm Simpson Gumpertz & Heger Inc. (SGH). His work
addresses issues related to the integrity and performance
of building enclosure systems on a range of structures,
including residential, commercial, institutional, and highrise
buildings. He has consulted with architects, contractors,
and building owners to analyze design concepts, evaluate
construction defects, and develop repairs for water intrusion
issues. He works in SGH’s Washington, DC, office.
Anthony J. Nicastro, PE
Abstracts for the 2013 RCI Symposium on Building Envelope Technology are being sought and should
be received at RCI headquarters by May 3, 2013. Potential authors/speakers will be notified by May 24
and will owe papers for peer review by July 19. RCI reserves the right of first publication of all submitted
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Topics of interest include innovative technologies and practices, façade systems and technologies,
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The symposium will be held November 14-15, 2013, at the Hyatt Regency in Minneapolis, MN.
For more information, contact RCI Director of Conventions and Meetings Karen McElroy
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